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1 article(s) from Hillier, Ian H

On the control of secondary carbanion structure utilising ligand effects during directed metallation

Andrew E. H. Wheatley,
Jonathan Clayden,
Ian H. Hillier,
Alison Campbell Smith,
Mark A. Vincent,
Laurence J. Taylor and
Joanna Haywood

Beilstein J. Org. Chem. 2012, 8, 50–60, doi:10.3762/bjoc.8.5

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Scheme 1: Molecular structures of 1/2-H and their corresponding ortho-lithiates [21].

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Scheme 2: Molecular structures of 3/4-H and their corresponding lateral lithiates [23,24].

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Scheme 3: Conversion of kinetic ortho-lithiate into the thermodynamic lateral lithiate under the influence of...

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Scheme 4: Molecular structure of 5-H and its lateral and ortho-lithiates [20].

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Scheme 5: Lateral metallation of 6-H using t-BuLi in the presence of Lewis base L.

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Figure 1: Molecular structure of 6-Li_l·PMDTA; H-atoms (excl. H8) omitted for clarity. Selected bond lengths (...

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Scheme 6: Comparison of aromatic and aryl–(α-C) bond distances in 5-Li_l·L [20] and 6-Li_l·L (L = PMDTA).

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Figure 2: Molecular structure of 6-Li_l·DGME; H-atoms omitted. Selected bond lengths (Å) and angles (°): O1–Li...

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Figure 3: Computed minimum energy conformers (B3LYP density functional/6-311++G(2d,2p) basis set; H-atoms omi...

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Published 09 Jan 2012

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